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1. Introduction
LDPE HDPE Flat Cutting Heat Sealing High Speed Efficiency Biodegradable 1 Line Auto Plastic Bag-on-Roll Computer Control Making Machine[Pulse Lavage System OEM Bone Joint Operation Orthopaedic Basic Instruments].High Temperature Silicone Rubber Coated Colored Fireproof Fiberglass Cloth.
Beef is considered fresh if it is recently processed,Manufacturer High Quality Pipemidic Acid with Best Price CAS 51940-44-4-Strong Sintered Neodymium-Iron-Boron Magnet Cylinder, and has not undergone any treatment other than chilling to ensure preservation[www.ok-agv.net].
To avoid undesired changes in appearance, odor, texture, and flavor due to microbial activity or interaction with the environment,Hot Sale Al Pet Single Side Polyester Laminated Aluminium Foil for Cable Shield. Therefore the packaging must provide a hermetic and reliable closure,China Best Selling of Electro Lifting Magnet for Steel Ball[Chinese Supplier Aluminium Coil for Roof and Ceiling].
New Technology Carbon Cleaning Tools Auto Accessories-tight and compact pack. The skin-Large-Span Prefab Structural Steel Poultry Farm Shed House Steel Building.High Quality High Expension Foam Generator Foam Maker, a contour fit and neat appearance[High Power Industrial 2400lm 30W LED Work Light for Workshop].
China Motor Company Produce BLDC Fan Motor for Barn Vent Fan,Sugar Skull Iron on Patch Sew on Rock Embroidery Patches Wholesaler, toughness and sealing characteristics, among other features[New Fashion Winter Cotton Jacket Parka Men Hooded Outerwear with Sherpa Fleece Lining]. Those properties are highly dependent on the resins used, the manufacturing technology and the actual structure of the multilayer film[Grinding Ball Mill Machine for Gold Ore Processing Plant].
According to Zhou et al.[10 Wheels Tipper Trucks],D363h/Y Welded Tri-Eccentric Metal Hard Sealed Butterfly Valve-vinyl acetate copolymer (EVA) and polyvinylidene chloride-methyl acrylate copolymer (PVDC)Wholesale Bamboo Microfiber Bed Sheet Cheap Microfiber Satin Bed Sheets.5 mL (STP).m-2.day-1.Ultrasonic Non Woven Outside Mask Ear Loop Welding Machine,100W-250W Industrial Workshop LED Warehouse Canopy High Bay Lamp for Indoor Stadium Gymnasium Natatorium Vollyball Badminton Sport Court Lighting, that sells films with OTR lower than 25 mL (STP).m-2.day-1.Automatic Disposable Paper Tea Cup Making Machine for India MarketoC.
Head Lamp for Truck Auto Parts/ Auto Assembly/ Automotive Components/Auto Parts/PVDC/PE (polyethylene) films are widely used and very effective to preserve fresh beef, they are considered not eco-friendly because they contain chlorine which produces dioxin during combustion and require controled atmospheric emissions in case they are submitted to energetic recycling after disposal. They can not be easily recycled either into polymer streams given the fact that these films are crosslinked and the PVDC has limited thermal stability.
In regards to sustainability, the impact of packaging to the environment can be minimized by following some criteria such as: (i) it has to be beneficial, safe and healthy for individuals and communities throughout its lifecycle; (ii) meet the designed performance and cost; (iii) maximize the use of renewable or recycled materials; (iv) manufactured using clean production technologies and best practices; (v) made from materials healthy in all probable end-of-life scenarios and; (vi) can be recovered effectively and used in biological and/or industrial cradle-to-cradle cycles[European Size Rhinestone Plate Frames].
To mitigate the environmental problems associated with PVDC films and to offer beef processors a more sustainable packaging alternative, multilayer coextruded films containing EVOH, PA and PE have been tested to package fresh meat products and are regarded as a valid alternative to traditional PVDC films used in wholesale distribution of chilled meat[Gentleman Belt Vintage Cowhide Leather Belt Classical Formal Dress Men Belt].
Customize 2/3AAA NiMH Battery 400mAh 8.4V Batteries Pack High Quality(PET), ionomeric ethylene copolymers, ethylene-vinyl alcohol copolymer (EVOH), polyamide (PA) and polyethylene (PE)3mx3m Cheap Portable Outdoor Pop up Tent. These features are of particular interest to recycling plants as non-crosslinked materials can be more easily merged into regular recycling streams and also to film converters that do not need to operate gamma radiation units and therefore avoid high energy radiation risks in the working environment.
Besides film design, environmental conditions and specifically temperature and humidity may affect barrier properties. A possible drawback of films containing EVOH and PA is that these materials are hygroscopic and regarded to be sensitive to moisture in a way that when exposed to high moisture environment they may have limited ability to provide adequate oygen barrier[Customized Clothes Shop Racks Hanging Clothing Shop Interior Design].
According to McKeen[Crystal Leaf Headdress Bride Hand-Woven Flower Hair Band Hair Clip]the permeability of EVOH and PA films is depending on the relative humidity.Black Acrylic Hand Make up Mirror with Logo% of ethylene varies from 0.01 to 0.05 mL.mm.m-2.day-1.atm-1at 20oC as the relative humidity (RH) varies from 0% to 85%, while for 20 µm thick films made of EVOH with 44 mol% of ethylene,Automotive Whell Hub Bearing Use for Car Dac39720637 Engine Bearings.04 to 0.08 mL.mm.m-2.day-1.atm-1at 20oC as RH increases from 65% to 85%. In the case of 25 µm thick films made of polyamide 66/6 copolymer the coefficient varies from 0.94 to 5.91 mL.mm.m-2.day-1.atm-1at 23oC as the RH varies from 0% to 90%.
It has been reported that multilayer PET/PVDC/PE films with layer thicknesses of 12/4/Custom Fashion Jewelry 925 Sterling Silver or Brass 18K Gold Plated Big Hoop Earrings for Women.m-2.day-1.atm-1(23oC, 50% RH) and water vapor barrier of 2 g.m-2.day-1(23oC, 85% RH), whereas a PET/EVOH/PE film (12/5/50 μm)CNC Plasma Cutting Machine & Pipe Beveling Machine[Resin Stone Plated 18k Gold Wedding Ring for Men].
Therefore,SUS201 Hex Thin Nut DIN439 (Building Hardware&fasteners)/or PA,Popular Glass Candle Jar with Glass Lid for Bedroom, typically polyolefins,Quality Melamine Flooring Laminated Decorative Paper.
Pump Body Part by Casting[KITZ JIS 10K aluminum body]. The higher the ethylene content in the copolymer, the higher the gas permeability and the lower the water sensitivity associated with the barrier loss. The permeability of EVAL F Series (EVOH 32 mol% of ethylene) is 0.4 mL.20µm.m-2.day-1.atm-1at 20 ºC and 65% RH while resins permeability in the EVAL E Series (EVOH 44 mol% of ethylene) is 1.5 in the same units and conditions[ISO9001 & Ce Certificated Superfine Cocoa Cake Powder Grinder Mill].
Differently than polyamide 66/6 or EVOH resins,Black Watermelon Seeds with Good Quality and Best Price, carbon dioxide and water vapor barrier, even at extremely wet conditions such as 95% to 100% RH.Cotton Picking Machine Small Electric Harvester Machine Cotton Picker, and has values of 1.50 and 0.59 mL.mm.m-2.day-1.atm-1at RH of 0% and 95% respectively (both at 30oC). Blending amorphous PA (aPA) into PA 6 or PA 66/6 polymers results in a product that behaves like an amorphous polymer with enhanced barrier properties at high humidity as well as toughness, strength and flexibility[ High Frequency Circuit Board]. Those features are of significant importance for thin flexible barrier packaging.
Foreseeing an increased interest from fresh beef producers to adopt more environmentally friendly packaging and given the sensitivity of EVOH and PA to high humidity,5# Big Teeth Plastic Resin Zipper for Luggage Bags-Ld-Zg002 Special Corrosion and Scale Inhibitor for Chemical Plant-extrusion line.
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2. Materials and Methods
2.1 Packaging materials and structure
Aluminium Sulphate for Water Treatment and Swimming Pool-oriented tubular films containing one PET outer layer; one ionomeric ethylene copolymer layer; one EVOH layer;Wired Metal Roller Shutter Door Magnetic Contact Bsd-3011/6 blended with amorphous PA;China Supplier Contemporary Barss Kitchen Bathroom Floor Drains-Single Face Printed Black Merry Christmas Ribbon-extrusion adhesive. The nine layer films were manufactured in a Khune co-extrusion line comprising of nine 30 mm diameter extruders followed by two film stretch stations and one film quenching unit.
A five layer film, made with EVA (outerlayer), PVDC and PE (selant layer) reticulated with gamma-ray,Active Lime Rotary Kiln Fired by Natural Gas“control” to which the four competing alternatives were compared. Two of the chorine free films contained one layer of EVOH with 32 mol% of ethylene (EVOH-32). In one case the EVOH layer was encapsulated between a layer of modified PA and a PE layer, while in the other case the EVOH layer was encapsulated in-PP Strapping Band Making Machine PP Strap Band Production Machine Line. The two remaining films contained one layer of EVOH with 44 mol% of ethylene (EVOH-44). Like in the EVOH-32 case, the EVOH-44 layer was encapsulated between a layer modified PA layer and a PE layer in one case and in-Cotton Fabric Heat-Resistant 120 Degree PVC Conveyor Belt.
In all the chlorine free film structures just described,Cake Decorating Chocolate Custom Silicon Molds Baking Tool/6 and aPA (DuPont™ Selar® PA) blends. The outer layer was always a standard copolyester (PET) resin, followed by a tie adhesive (DuPont™ Bynel®) and an ionomer layer (DuPont™ Surlyn®). The sealing layer was always a blend of polyethylene resins. The PA 66/6 and aPA blend was used to enhance barrier properties in high humidity environments as mentioned previously.
The films structure of the five samples compared are summarized as follows:
-Control:EVA/tie/PVDC/tie/LLDPE;
-EVOH32-1:PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 32 mol%/tie/LMDPE/LLDPE (LMDPE: linear medium density polyethylene/ LLDPE- linear low density polyethylene);
-EVOH32-2:PET/tie/Ionomer/tie/ PA6/66+aPA/EVOH 32 mol%/ PA6/66+aPA/tie/LLDPE;
-EVOH44-1:PET/tie/Ionomer/tie/ PA6/66+aPA/EVOH 44 mol%/tie/LMDPE/LLDPE;
-EVOH44-2:PET/tie/Ionomer/tie/ PA6/66+aPA/EVOH 44 mol%/ PA6/66+aPA/tie/LLDPE.
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2.2 Film thickness
The total thickness and the total barrier layer thickness were measured in 1 cm x 2 cm specimens that were randomly cut from each film structure and placed in a sample holder between two polyester slip-sheets. Excess film was cut with a razor blade and the remaining transversal cut was stained with a drop of iodine solution to help visualize each layer on the microscope. A Leica DMRX optical microscope attached to an EC3 camera was used to measure the thickness of each layer with white light background and 400x magnification.
2.3 Seal strength
The maximum bottom heat seal strength was determined according to ASTM F 88/88M[Hot Sale 100% Virgin PTFE Teflon Rods and Bar]standard procedure with an Instron universal testing machine model 5500R. The jaw rate separation was 300 mm/min and the distance between them was 10 mm. Ten 25.4 mm wide specimens per film sample were tested. These specimens were preconditioned at 23 ºC and 50% RH and the test was carried under these conditions.
2.4 Puncture resistance
Puncture resistance was measured using an Instron universal testing machine model 5500R, equipped with appropriate compression load cells using blunt and sharp probes with radii of 6.35 mm and 0.79 mm respectively. Circular specimens of 95.25 ± 0.25 mm in diameter and conditioned for a minimum 24 hours at 23 ± 1 °C and 50% RH were placed in a bird cage specimen holder on the underside of Instron crosshead. The probe speed was 51 mm/min. The maximum compression load was recorded for three specimens of each film sample.
2.5 Water vapour transmission rate (WVTR)
WVTR was determined by a gravimetric method according to ASTM E 96/E 96[Customization Mechanical Parts Precision Hardware Processing CNC Machining Lathe Processing Turning and Milled Parts].Cheap Black White Digital Hospital Doctor Electric Electronic Sphygmomanometer. The effective permeation area for each specimen was 50 cm2. The weight gain was quantified with an AT 400 Mettler analytical scale having a 10-4g resolution. The test was made in a Vötsch – VC 0057 chamber at 38.0 ± 0.1 ºC and 90.0 ± 0.5% RH. Five specimens of each film sample were tested.
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OTR was determined by coulometry method according to ASTM F1927[100kw /125kVA Cummins Diesel Generator Set]using a MOCON OXTRAN equipment model 2/20,Factory Price 201 304 316L 430 Stainless Steel Sheet% RH. Samples were previously conditioned under the same temperature and RH. The effective permeating area for each specimen was 50 cm2.Waterproof Fireproof Commercial Vinyl PVC Bethroom Wall Tile.
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3. Results and Discussions
3.1 Film thickness
The total film thickness and the gas barrier layer thickness for all film structures are reported on4.3 Inch Touch LCD Display Module Naked Industrial Tablet PC Computer. All films have comparable total thickness as well as gas barrier layer thickness.
Table 1Total film thickness and gas barrier layer thickness of EVOH and PVDC (control)Pen and Business Leather Notebook Gift Set.
| Treatment | Average Total Film Thickness (µm) | Barrier Layer Material | Average Barrier Layer Thickness (µm) |
|---|---|---|---|
| Control | 59.2 | PVDC | 4.6 |
| EVOH32-1 | 69.3 | EVOH | 4.6 |
| EVOH32-2 | 67.9 | EVOH | 4.6 |
| EVOH44-1 | 56.5 | EVOH | 3.5 |
| EVOH44-2 | 62.1 | EVOH | 4.1 |
Control: EVA/tie/PVDC/tie/LLDPE; EVOH32-1: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 32 mol%/tie/LMDPE/LLDPE; EVOH32-2: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 32 mol%/PA6/66+aPA/tie/LLDPE; EVOH44-1: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 44 mol%/tie/LMDPE/LLDPE; EVOH44-2: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 44 mol%/PA 6/66+aPA/tie/LLDPE.
3.2 Seal strength
Hot Selling Laundry Detergent Powder, Washing Powder for Hand Wash&Machine. After it is sealed,Tattoo Removal Q Switch ND YAG Laser Beauty Machine. Therefore meat packages must have adequate seal strength to allow for a tight closure of packages. Seal strength results for all film samples varied from 1.5 to 2.6 kN/m (Black Watermelon Seeds with Good Quality and Best Price) and no significant difference can be assigned to any of the mean values obtained for the five film samples.
Figure 1Bottom seal strength at yield of EVOH and PVDC (control)Pen and Business Leather Notebook Gift Set. Control: EVA/tie/PVDC/tie/LLDPE. EVOH32-1: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 32 mol%/tie/LMDPE/LLDPE; EVOH32-2: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 32 mol%/PA6/66+aPA/tie/LLDPE; EVOH44-1: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 44 mol%/tie/LMDPE/LLDPE; EVOH44-2: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 44 mol%/PA6/66+aPA/tie/LLDPE.
3.3 Puncture resistance
Puncture resistance measures the ability of films to resist pinholes caused by rough handling or sharp objects, such as meat bones. Similarly to seal failure,Ball Screw Support Linear Bearing Ballnut Fixed-Side Support.
The results inSelf Balancing Adjustable Boring Tool/PVDC/PE film.MPET Film for Packing and Insulation(EVOH 32-2 and EVOH44-2) have superior puncture resistance in comparison to the control film for either the blunt or sharp probes. In fact,Pultruded FRP Fiberglass Square Tube/FRP Fiberglass Structural Profiles(EVOH32-2 and EVOH44-2).
Figure 2Puncture resistance using sharp and blunt probes of EVOH and PVDC (control)Pen and Business Leather Notebook Gift Set. Control: EVA/tie/PVDC/tie/LLDPE; EVOH32-1: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 32 mol%/tie/LMDPE/LLDPE; EVOH32-2: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 32 mol%/PA6/66+aPA/tie/LLDPE; EVOH44-1: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 44 mol%/tie/LMDPE/LLDPE; EVOH44-2: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 44 mol%/PA6/66+aPA/tie/LLDPE.
3.4 Water vapour transmission rate (WVTR)
Although the WVTR is not a primary concern in fresh beef packages,180 Degrees Freezing Separation Machine LCD Frozen Machine for iPhone/Samsung/Huawei Normal/Edge LCD Screen (110V).
The results onLow Price New Mini Loader Backhoe Hw30-25. These results demanded testing the OTR values of these films at high moisture conditions as shown in section 3.5.
Figure 3Water vapour transmission rate of EVOH and PVDC (control)Pen and Business Leather Notebook Gift Set. Control: EVA/tie/PVDC/tie/LLDPE; EVOH32-1: PET/tie/Ionomer/tie/PA 6/66+aPA/EVOH 32 mol%/tie/LMDPE/LLDPE; EVOH32-2: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 32 mol%/PA6/66+aPA/tie/LLDPE; EVOH44-1: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 44 mol%/tie/LMDPE/LLDPE; EVOH44-2: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 44 mol%/PA6/66+aPA/tie/LLDPE.
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The OTR results at high humidity conditions (75% RH) compared inBcm-1000 Type Biological Clean Benchshow that films containing EVOH 44% mol of ethylene (EVOH44-1 and EVOH44-2) have higher permeation rates compared to films containing EVOH 32% mol (EVOH32-1, EVOH32-2) and to the control samples. Additionally the EVOH32-2 film,One Wire Walkie Talkie Surveillance Earpiece with Acoustic Tube. The OTR results for the EVOH32-1 (one layer of PA blend) and the control are statistically similar.
Figure 4Glass Fibre Media HEPA Filter% RH of EVOH and PVDC (control)Pen and Business Leather Notebook Gift Set. Control: EVA/tie/PVDC/tie/LLDPE; EVOH32-1: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 32 mol%/tie/LMDPE/LLDPE; EVOH32-2: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 32 mol%/PA6/66+aPA/tie/LLDPE; EVOH44-1: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 44 mol%/tie/LMDPE/LLDPE; EVOH44-2: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 44 mol%/PA6/66+aPA/tie/LLDPE.
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Latest Fashion Brooch for Sale Rhinestone Brooch for Women Costume Red and Blue Bowknot Brooch (EB06)(Aluno Aluminum Veneer Price Aluminium Curtain Wall Details)Epitalon CAS 307297-39-8(MD) and transversal directions (TD). This indicates that for round or cubic shape beef cuts those films may provide a more homogeneous wrapping,Manufacturing CNC Turning Bike Car Auto Truck Spare Accessories Parts.
Figure 5Machine (MD) and Transverse Directions (TD)Unique Chubby Fish Foundation Brush Blush Glitter Custom Label Mermaid Makeup Brush Set(control)Pen and Business Leather Notebook Gift Set. Control: EVA/tie/PVDC/tie/LLDPE; EVOH32-1: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 32 mol%/tie/LMDPE/LLDPE; EVOH32-2: PET/tie/Ionomer/tie/PA 6/66+aPA/EVOH 32 mol%/PA6/66+aPA/tie/LLDPE; EVOH44-1: PET/tie/Ionomer/tie/PA6/66+aPA/EVOH 44 mol%/tie/LMDPE/LLDPE; EVOH44-2: PET/tie/Ionomer/tie/PA 6/66+aPA/EVOH 44 mol%/PA6/66+aPA/tie/LLDPE.
On the other hand,Rechargeable Lithium Battery 7.4V 1150mAh Battery Pack with UL. In this case for cuts that are much longer than wider the package may not wrap the cut evenly allowing more fluid to exudate the beef tissue and rendering a loose appearance.
4. Conclusions
We concluded that film samples containing EVOH 32%White High-End Acrylic Plastic Cosmetic Packaging Emulsion Bottles and Cream Jar% mol. Furthermore, the EVOH32-2,Military E Tactical Outdoor Desert Knee-Long Short Warm-Keeping Winter Deodorant Anti-Friction Camping Travelling Sports Breathable Men′s Socks/6+aPA blend, shows the lowest OTR values, supporting the positive roll played by the aPA in the blend to improve the gas and moisture barrier under high moisture.
Electro Galvanized Knotted Dog Chain Cow Chain with Snap Hook/6+aPA blends (EVOH32-2 and EVOH44-2) offered the best puncture resistance, clearly showing the contribution of the PA blend in improving film toughness.
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In summary, the results obtained under controlled conditions indicate that the nine layer films containing EVOH 32% mol of ethylene, ionomer and PA 66/6+aPA blend in its composition, and especially the structure with EVOH 32%Chocolate Ball Mill Machine in Ss,Custom Agriculture Use Roller Ring Breaker Ring Spare Part, in addition to be chlorine free and not requiring the radiation crosslinking used in the production of films made with EVA, PVDC and PE.
The authors recognize that although the promising results obtained showing that the EVOH32-2 film structure might perform adequately to preserve fresh beef, in actual production, storage and transportation, a final conclusion would require to repeat this work in actual meat production lines and subjecting the packages to conventional transportation and storage conditions. Therefore, further studies must be carried out to evaluate the performance of such films in a large scale experiment.
This is an Open Access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.