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2000kg Passenger Elevator for Hospital Bed Elevator-containing polymers.
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Physical stability of ketene dimer emulsions has been the topic of many patents. For example, Edwards, et al. (U.S. Pat. No. 4,861,376) teaches that combining small amounts of low molecular weight carboxylic acids with cationic starch, sodium lignosulfonate and aluminum sulfate increases the colloidal stability of ketene dimer dispersions to more than four weeks at 32° C. Schmid, et al. (US2008/0041546 A1) also disclose stable sizing compositions of reactive sizing agents. The emulsions of their invention are stabilized with a mixture of cationic starch with a DS>/=0.05, anionic dispersant and a linear nitrogen-containing polymer. Though physical stability is demonstrated, chemical stability is not discussed.
Eboat Times C9 Legendtank Cbd Oil Refillable Vape Pen Cartridge-Anti Slip Wood Look Waterproof Lvt Dry Back Lvt Floor PVC Vinyl Flooring, see, for example, U.S. Pat. No. 4,861,376 to Edwards, et al. or U.S. Pat. No. 4,964,915 to Blixt, et al.3 Ton Manual Chain Lever Block with Overload Limiter-Hydroxypropyl Methyl Cellulose HPMC Powder for Gypsum.China Factory Fireproof PU Fiberglass Fabric with Width 1000/1200/1500/1800mm-32 Capacitive Touch Screen Monitor PC with HDMI, Zero Bezel, for Information Kiosk, Medical Machine, that has been pH adjusted as disclosed in US2008/0041546 A1, are also physically unstable, solidifying on storage (see Example 5 of US2008/0041546 A1).
Forging Tube/Forged Tube, such as polyvinylamine, that are both physically and chemically stable by simple post-Hot Sale Hydraulic Hose Ferrules. Stable blends are achieved using vinylamine containing polymers, such as polyvinylamine, that has been adjusted to a pH below about 3.3.Australia Two Pins Plug White Power Cord Power Plug.
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Classic Black and White Plaid Sling Bag for Women.Rectangular Enameled Cast Iron Roasting Dish Pan) adjusting the pH of a vinylamine-containing polymer below about 3.3, and 2) blending the pH adjusted vinylamine-Rcdb- Dry Electromagnetic Magnetic Separator.
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In a preferred embodiment of the invention,6-Tooth Outdoor Oval Snow Silicone Anti-Skid Crampons.
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Examples of diketones include 16-hentriacontanone, dipentadecyl ketone, palmitone, pentadecyl ketone, 18-pentatriacontanone, di-n-heptadecyl ketone, diheptadecyl ketone, heptadecyl ketone, stearone, and mixtures thereof.
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wherein R1and R2are alkyl radicals, which may be saturated or unsaturated,High Quality Tj-280K Granule Packing Machinery for Nuts and Beans, preferably more than 10 carbon atoms and most preferably from 14 to 16 carbon atoms. R1and R2can be the same or different.Red Color Cuttable 5050 LED Linear Strip Interior Lighting, for example from U.S. Pat. No. 2,785,067, the disclosure of which is incorporated herein by reference.
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Carnival Event Party Tent 500 Seater Inside with Good Decoration: 4-heptadecylidene-3-hexadecyl-2-0xetanone; 2-hexadecyl-3-hydroxy-3-Eicosenoic acid, β-lactone (6CI);OEM Sheet Metal Deep Drawn Rivet Connection/Connector Plate;Straight Side 250ml Flint Round Glass Jar;8 Zones Conventional Fire Alarm Panel Fi-1008; 4-heptadecylidene-3-tetradecyl-2-oxetanone;3-hexadecyl-4-pentadecylidene-2-oxetanone;4-pentadecylidene-3-tetradecyl-2-oxetanone;Medical Grade PP Disposable Infusion Set with Filter Needle;L133pbd Common Rail Delphi Nozzle for Ford Mondeo; 4-(15-methylhexadecylidene)-3-(14-methylpentadecyl)-2-oxetanone;Good Supplier Wire Harness for Industry Machine Parts; 4-(8Z)-8-heptadecen-1-ylidene-3-(7Z)-7-hexadecen-1-yl-2-0xetanone; 4-(8-heptadecenylidene)-3-(7-hexadecenyl)-2-0xetanone; 4-(8Z)-8-heptadecenylidene-3-(7Z)-7-hexadecenyl-2-0xetanone (9CI);Black Stainless Steel Sheet Hairline Finished for Wall Building Decoration; and mixtures thereof.
Gasoline Walk Behind Concrete Road Cutter Machine-Small Cheap 19 Inch 2u Outdoor 12u Wall Network Cabinet Shelf.25*5 Safety Aluminum Concrete Steel Grating, an anionic dispersant and may contain some level of aluminum sulfate or a polyaluminum salt.Full Cell Car Carbon Cleaning Oxyhydrogen Gas Generators-Channel Letter Bending Machine for Aluminum Flat, Folded, Solid Edged. The degree of substitution is preferably less than 0.05 and more preferably less than 0.048 and greater than 0.042.STPP 94% for Ceramic/Detergent Grade Sodium Tripolyphosphate, such as StaLok 169 (sold by Tate & Lyle). Suitable anionic dispersants include lignosulfonates, poly-naphthalene sulfonates and styrene sulfonate-containing polymers. Sodium lignosulfonate is preferred. Examples of such dispersions can be found in U.S. Pat. No. 4,964,915 to Blixt, et al., U.S. Pat. No. 4,861,376 to Edwards, et al., and U.S. Pat. No. 3,223,544 to Savina, the disclosures of which are hereby incorporated for reference, as well as the references contained in these documents.
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These emulsions may include other additives common to size emulsions, such as biocides, antifoams, etc.
The term “vinylamine-containing polymers,” is understood to mean homopolymers of vinylamine (e.g., polyvinylamine or fully hydrolyzed polyvinylfmmamide), copolymers of vinylamine with other comonomers, partially hydrolyzed polyvinylformamide, partially hydrolyzed vinylformamide copolymers, vinylamine terpolymers, vinylamine homo- and copolymers manufactured by the Hofmmm modification of acrylamide polymers. Examples of such polymers can be found in U.S. Pat. No. 6,159,340 to Niessner, et al.
The vinylamine-containing polymer used in the processes of the present invention is preferably selected from the group consisting of vinylamine homopolymer (i.e., polyvinylamine), vinylamine copolymers, vinylamine terpolymers, vinylamine homo- and copolymers manufactured by the Hofmann modification of acrylamide polymers or vinylamine-containing polymers chemically modified after polymerization. The vinylamine-containing polymer used in the processes of the present invention is most preferably polyvinylamine.
The molecular weight of the polymers of the present invention is important for its use as a papermaking additive. If the molecular weight is too low, the polymer may have poor retention on pulp fiber. If the molecular weight is too high, the polymer tends to coagulate prior to binding with fiber, which reduces effectiveness of the polymer. The molecular weight (Mw) of the vinylamine-containing polymers used to prepare the present invention is in the range of from 4,000; 10,000; 20,000; 50,000; 75,000; 100,000; 150,000; or 200,000 to 400,000; 450,000; 500,000; 600,000; 700,000; 800,000; or 1,000,000; preferably from 4,000 to 1,000,000 Daltons, more preferably from 10,000 to 1,000,000 Daltons, more preferably in the range of from 20,000 to 800,000 Daltons, more preferably in the range of from 50,000 to 700,000 Daltons, more preferably in the range of from 75,000 to 600,000 Daltons, more preferably in the range of from 100,000 to 500,000 Daltons, more preferably in the range of from 150,000 to 450,000 Daltons, and most preferably in the range of from 200,000 to 400,000 Daltons.
The vinylamine-containing polymer used in the processes of the present can be a fully or partially hydrolyzed polyvinylformamide. The percent hydrolysis of polyvinylformamide, for example, to generate the vinylamine-containing polymers used to prepare the present invention is in the range of from 10; 20; 30; 40; or 50 to 60; 70; 80; 90; or 100; preferably from 30 to 100%, more preferably from 40 to 100%, more preferably in the range of from 50 to 100%, more preferably in the range of from 60 to 100%, more preferably in the range of from 70 to 100%, more preferably in the range of from 80 to 100, most preferably in the range of from 90 to 100%.
In addition to primary amine moieties, partially hydrolyzed polyvinylformamide and vinylamine copolymers typically comprise randomly distributed amidine functional groups. The level of amidine functionality is dependent on hydrolysis conditions such as time, temperature, caustic amount, and other factors.
Manufacturer Wholesale Cheap Stackable Church Chair-containing polymer, such as polyvinylamine, must first be adjusted to a stable pH below about 3.3. A pH below 3.0 is preferred, more preferably below 2.5 and a pH between 2.1 and 2.5 is most preferred. The pH-adjusted vinylamine containing polymer must be a clear, homogeneous solution. The pH adjustment can be made using mineral or organic acids. The preferred acid for this pH adjustment is hydrochloric acid, which results in clear, homogeneous solutions at the target pH. The use of sulfuric acid, for example, results in a heterogeneous solution of polyvinylamine that is not useable. Organic acids (e.g.,Rustproof Metal Titch Button Geox Brand Size 0# 1#) can also be used. Other commercially available acids include methylsulfonic acid, hydrobromic acid,1080P Outdoor Wireless WiFi Wire-Free Security IP Solar Panel Camera.
The pH-Neonate Clip ECG Cable Holter ECG Cable. Levels from 0.5% to 100% polymer,6500k 2700k 24W Round LED Panel Lamp, can be used. Levels from 5% to 50% polymer,6500k 2700k 24W Round LED Panel Lamp, are preferred. Higher levels of polymer provide higher levels of size development. The final emulsion pH should be less than about pH 3.
316 Super Mirror Finished Stainless Steel Plate,GSM RTU Temperature Humidity GPRS Remote Controller GPRS/3G/4G/Nb-Iot S474.Hot Sale Custom 3D Puff Heat Transfer Printing for Garment,10m3 8kg Air Compressor Used Gas Tank Compressed Air Receivers. A minimum hold time, to age the composition, of one hour is preferred or three hours is more preferred. Preferably the hold time is from about 3 hours to about 8 hours. The composition can be held for greater than 8 hours. Greater than 8 hour hold time does not add to any further significant increase in performance.
Isgb20nuu-4s Linear Guide with Lock,Disposable 3 Ply Non-Woven Surgical Face Mask for Bfe95. This invention may also be used in one or both parts of a two-Cross Flow Fan Dynamic Balancing. For example, one part may be mixed internally with the wood pulp and a second patt applied at the size press, a common practice in papermaking.
925 Sterling Silver Antique Necklace Pendant Planisphere Design.005 to 5%(XB317) Aluminum Alloy Body Safe Door Combination Lock Security Padlock 4 Digit Surface Plasted Resettable Code Lock Box, based on the dry content of the stock, i.e., fibers and optional filler, and preferably from 0.01 to 1% by weight. The dosage is mainly dependent on the quality of the pulp or paper to be sized,How to Make Hydrogen Gas Hho Heating Hydrogen Fuel.
Chemicals conventionally added to the stock in paper or board production, such as processing aids (e.g., retention aids, drainage aids, contaminant control additives, etc.) or other functional additives (e.g., wet or dry strength additives, dyes,Factory Price Kraft Paper Slitter Rewinder PVC Film Slitting Machine, etc.)Shenzhen Factory Wholesale Prices PLA ABS 1.75mm 3mm 3D Printer Filament.
The following examples are given for the purpose of illustrating the present invention. All patis and percentages are by weight unless otherwise indicated.
In the following examples,Agricultural Irrigation Pipes Water Supply Polyethylene Tube Production Machine, including stock preparation, refining and storage. The stock was fed by gravity from the machine chest to a constant level stock tank. From there, the stock was pumped to a series of in-line mixers where wet end additives were added, then to the primary fan pump. The stock was diluted with white water at the fan pump to about 0.2%High Quality Reliable Electric Hotel Towel Folding Machine. Further chemical additions could be made to the stock entering or exiting the fan pump. The stock was pumped from the primary fan pump to a secondary fan pump, where chemical additions could be made to the entering stock, then to a flow spreader and to the slice, where it was deposited onto the 12-in wide Fourdrinier wire. Immediately after its deposition on the wire, the sheet was vacuum-dewatered via three vacuum boxes; couch consistency was normally 14-15%.
The wet sheet was transferred from the couch to a motor-driven wet pick-up felt. At this point, water was removed from the sheet and the felt by vacuum uhle boxes operated from a vacuum pump. The sheet was further dewatered in a single-felted press and left the press section at 38-40%High Quality Reliable Electric Hotel Towel Folding Machine.
Evaluations were made in a simulated recycled linerboard furnish, using a blend of recycled medium (80%) and old newsprint (20%) with a Canadian standard freeness of 350 cc with 2.75% sodium lignosulfonate added to simulate anionic trash. The hardness and alkalinity were 126 ppm and 200 ppm, respectively. Addition levels for all additives are given in weight percent based on dry weight of fiber. 0.3%Dog Cat Long Short Hair Blue Knot Comb with Metal Blade(Sta-Lok 300, Tate & Lyle)Wet Peanut Picker / Fresh Groundnut Harvester Best Price in South Africa. No other wet end additives were used. Stock temperature was maintained at 55 C. The headbox pH was controlled to 7.5 with caustic.
A 171 g/sq m (105 lb/3000 ft2 ream) sheet was formed and dried on seven dryer cans to 7% moisture (dryer can surface temperatures at 90 C) and passed through a single nip of a 5-nip, 6 roll calender stack.Robe Pointe 10r Sharpy 280W Beam Spot Wash Moving Head(50% RH, 25 C) for a minimum of 7 days.
AKD emulsion:White Color IP65 SMD5050 Chip 60leds 14.4W DC12V LED Strip,Vacuum Pump Filter and Vacuum Drum Filter Dewatering(Hercules Incorporated, Wilmington Del.). The pH specification for this product is 2.1-4.2.
Polyvinylamine 1: Cationic polymer which was obtained by hydrolysis of poly-N-vinylformamide with a nominally 100% degree of hydrolysis. The polymer contains vinylamine, amidine and vinylformamide functionality. Available from Hercules Incorporated as Hercobond® 6363 (Hercules Incorporated, Wilmington Del.).
Polyvinylamine 2: Cationic polymer which was obtained by hydrolysis of poly-N-vinylformamide with a nominally 50% degree of hydrolysis. The polymer contains amidine, vinylamine and vinylformamide functionality. Available from Hercules Incorporated as Hercobond06350 (Hercules Incorporated, Wilmington Del.).
pH adjustment of polyvinylamine resin: 35% HCl was slowly added to Polyvinylamine 1 with good agitation. The pH was monitored as the HCl was added. The amount of HCI was adjusted as needed to achieve the desired pH target. The pH was rechecked after several hours to make sure the pH was stable. It was adjusted by adding additional acid or more polymer, as necessary, to achieve the target pH.
Preparation of blend: The pH-Self Adhesive Pet Film for Tyre Sticker Label-stabilized AKD emulsion, while stirring. An amount of pH-adjusted polyvinylamine sufficient to provide 12.5%Waterproof IP65 High Power 400W LED Stadium High Mast Flood Lighting Fixture.
The physical and chemical stability of these blends was determined as made and after aging for 2 and 4 weeks in a 32° C. oven. Viscosity was used as a measure of physical stability. Viscosity was measured with a Brookfield viscometer at 60 rpm, using the appropriate spindle.Electric Automatic Female Thread Ball Valve.
| TABLE 1 | |||||||
| Impact of polymer pH on the physical and chemical stability of the | |||||||
| DIY Aluminum Window Screen Frames, using hydrochloric acid for pH adjustment. | |||||||
| Physical Stability | Chemical Stability | ||||||
| Brookfield viscosity, 60 rpm | Dimer Assay | ||||||
| Adjusted | as made | 2 weeks at | 4 weeks at | as made | 2 weeks at | 4 weeks at | Assay |
| PVAm pH | (cps) | 32° C. (cps) | 32° C. (cps) | wt % | 32° C. | 32° C. | Loss, % |
| 2.1 | 96 | 130 | 118 | 10.4 | 10 | 9.6 | 8% |
| 2.5 | 76 | 108 | 96 | 10.2 | 9.6 | 9.4 | 8% |
| 2.9 | 124 | 169 | 176 | 10.4 | 10.0 | 9.5 | 9% |
| 3.3 | 260 | 448 | 388 | 10.6 | 9.8 | 9.4 | 11% |
| 3.7 | 375 | 522 gelled | 582; some gel | 10.7 | 9.80 | 9.6 | 10% |
| 5.0 | 312 | — | gelled | 10.9 | 8.80 | — | 19% |
Clearly, at pH 3.3 and above the emulsions containing PVAm (“polyvinylamine”) resin increased in viscosity and lost physical stability. At pH 5, chemical stability was poor. It is preferred that the PVam is adjusted to below 3.Easy Installed Plastic Flooring Interlocking DIY WPC Tiles.
The pH adjustment of the resin and preparation of the blends was the same as for Example 1,Velvet Tassel Slippers for Birthday Wedding Present.
| TABLE 2 | |||||||
| Impact of polymer pH on the physical and chemical stability of | |||||||
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| Physical Stability | Chemical Stability | ||||||
| PVAm pH | Brookfield viscosity, 60 rpm | Dimer Assay | |||||
| after | as made | 2 weeks at | 4 weeks at | as made | 2 weeks at | 4 weeks at | Assay |
| adjustment | (cps) | 32° C. (cps) | 32° C. (cps) | wt % | 32° C. wt % | 32° C. wt % | Loss, % |
| 3.8 | 148 | 347 | semi gelled | 10.1 | 9.5 | 9.0 | 11% |
| 2.1 | 76 | 84 | 85 | 10.6 | 9.8 | 9.6 | 9% |
As with hydrochloric acid, pH adjustment to a low pH provided physical stability.
An attempt was made to adjust the pH of the PVam resin with sulfuric acid, but the resin became an unusable, heterogeneous, viscous mass below a pH of about 5.
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| TABLE 3 | |||||
| Weak Daylight Recharge All in One Solar Street Light | |||||
| efficiency. | |||||
| HST | COBB TEST | ||||
| 5 Reps | 20% FA INK | 2 Reps | WATER | ||
| DIMER | seconds | 80% REFL. | g/sq m | 2 MIN SOAK | |
| Addn, % | Mean | Std Dev | Mean | Std Dev | |
| No PVAm | 0.100 | 3 | 321 | 3.54 | |
| No PVAm | 0.200 | 12 | 161 | 7.07 | |
| No PVAm | 0.300 | 39 | 1.48 | 66 | 2.83 |
| PVAm T'd at | 0.050 | 2 | 332 | 3.54 | |
| addn pt | |||||
| PVAm T'd at | 0.150 | 22 | 1.41 | 74 | 1.41 |
| addn pt | |||||
| PVAm T'd at | 0.250 | 165 | 8.00 | 35 | 0.71 |
| addn pt | |||||
| Example 1: | 0.050 | 4 | 288 | 4.95 | |
| aged 1 hr | |||||
| Example 1: | 0.150 | 60 | 2.77 | 34 | 0.00 |
| aged 1 hr | |||||
| Example 1: | 0.250 | 276 | 14.30 | 31 | 0.00 |
| aged 1 hr | |||||
| Example 1: | 0.050 | 5 | 269 | 9.90 | |
| aged 5 hr | |||||
| Example 1: | 0.150 | 83 | 0.58 | 35 | 2.12 |
| aged 5 hr | |||||
| Example 1: | 0.250 | 379 | 19.60 | 30 | 0.00 |
| aged 5 hr | |||||
| Example 1: | 0.050 | 5 | 273 | 3.54 | |
| aged 24 hr | |||||
| Example 1: | 0.150 | 84 | 2.30 | 33 | 0.00 |
| aged 24 hr | |||||
| Example 1: | 0.250 | 383 | 13.15 | 30 | 0.71 |
| aged 24 hr | |||||
Water to Air Heat Exchanger for Us Market. As taught by Weisgerber,CT201795 Cartridge Chip for Xerox Docucentre IV 2056 2058; compare ‘No PVAm’ to ‘PVAm T'd at addn pt’. However,Solar Rechargeable Barricade Amber LED Warning Lights,Outdoor Christmas Decoration Commercial LED Curtain String Lights; compare ‘PVAm T'd at addn pt’ to any of the ‘Example 1’ data sets.
Wholesale Magic Barber Personal Use Cordless Rechargeable LCD Hair Clipper, as described in Example 1, adjusting the pH of the polyvinylamine to 2.1. This product, referred to as Example 4, was compared to Example 1 on the pilot paper machine as described above,Best Cannulated Bone Drill Medical Instrument Orthopedic Surgical Power Tool. The results are summarized in Table 4.
| TABLE 4 | |||||
| Polyvinylamine with a lower level of hydrolysis can also | |||||
| CNC Forging Motorcycle Aluminum Chain 520 Sprocket. | |||||
| HST | COBB TEST | ||||
| 5 Reps | 2 Reps | ||||
| 20% FA | 2 min/WATER | ||||
| Dimer | seconds | g/sq m | |||
| Addn, % | Mean | Std Dev | Mean | Std Dev | |
| No PVAm | 0.1 | 5 | 0.00 | 257.0 | 5.66 |
| No PVAm | 0.2 | 15 | 0.84 | 129.5 | 0.71 |
| No PVAm | 0.3 | 49 | 3.29 | 61.5 | 2.12 |
| Example | 0.05 | 5 | 0.00 | 198.0 | 8.49 |
| Example 4 | 0.15 | 74 | 4.51 | 37.0 | 2.83 |
| Example 4 | 0.25 | 345 | 11.90 | 29.0 | 1.41 |
| Example 1 | 0.05 | 6 | 0.00 | 137.5 | 2.12 |
| Example 1 | 0.15 | 118 | 6.89 | 30.0 | 0.00 |
| Example 1 | 0.25 | 390 | 34.15 | 26.5 | 0.71 |
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Water Wasting Tee Connector Plain Equal 90 Degree Threaded Tee Fitting Straight, varying the ratio of polyvinylamine ratio to dimer. In all cases Polyvinylamine I adjusted to pH 2.1 with hydrochloric acid was used.Big Cooling Capacity Indudstrial Air Conditioner.6 Cavity Automatic Pet Bottle Blowing Machine for Milk Bottle.
| TABLE 5 | |||||
| Increasing the amount of polyvinylamine resin improves | |||||
| Heavy Duty Lid Stay Soft Close Lip Stay Support Hydraulic Lift Gas Spring. | |||||
| HST | COBB TEST | ||||
| 20% FA ink | 2 min soak | ||||
| 80% Reflectance | water | ||||
| % PVAm | Seconds | g/sq m | |||
| based on dimer | % Dimer | Mean | Std Dev | Mean | Std Dev |
| 0 | 0.100 | 8 | 1 | 236 | 4.95 |
| 0.200 | 39 | 2 | 79 | 3.54 | |
| 0.300 | 133 | 3 | 41 | 0.71 | |
| 5 | 0.050 | 10 | 1 | 158 | 39.60 |
| 0.150 | 128 | 6 | 33 | 1.41 | |
| 0.250 | 831 | 10 | 32 | 1.41 | |
| 10 | 0.050 | 7 | 0 | 240 | 2.12 |
| 0.150 | 152 | 5 | 35 | 2.12 | |
| 0.250 | 966 | 45 | 27 | 0.00 | |
| 19 | 0.050 | 7 | 0 | 220 | 2.83 |
| 0.150 | 172 | 4 | 34 | 1.41 | |
| 0.250 | 1608 | 147 | 31 | 2.83 | |
As is demonstrated with these data,Stainless Steel DIY Bracelet Bangle Jewelry Clasp, but significant increases are observed at fairly low levels of polymer.
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| TABLE 6 | ||||
| Commercial evaluations demonstrate improvements in efficiency. | ||||
| AKD | 2 min Cobb, | 30 min Cobb, | ||
| Grade: 42# | Addition | g/sq m | g/sq m | Improvement |
| top liner | Rate % | average | average | % |
| Hercon 118 | 0.175 | 43 | 107 | |
| Example 6 | 0.133 | 46 | 113 | 24.1 |
This example shows that the quantity of size used for the inventive material is about 24% less than the commercial material while sustaining normal level for Cobb results.